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The simplest way of measuring the concentrations in the two phases is to read the absorbance by a spectrometry method Unfortunately, spectrometric methods are suited only for compounds that either are very pure or have unique chromophores For most pharmaceutical compounds at discovery stage, it is dif cult to obtain pure compounds A separation technique, such as HPLC, can avoid interferences from impurities, eliminating the purity and/or unique chromophore requirements,15 and allow for UV/Vis detection Even with HPLC separation, UV/Vis detection still has its limitations First, even with photodiode array (PDA), UV/Vis may be not speci c enough to identify co-eluting impurities, especially when the concentration of the sample is relatively low or the compound of interest has low absorbance Second, it is very hard to identify the peak of interest when there are multiple peaks An example is shown in Figure 17.

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